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Thus collected carbon was ball milled using a vibratory ball mill, 8000D mixer/mill from SPEX SamplePrep, with Zirconia vials and balls. Two separate zirconia ceramic vials of 45 ml (6.35 cm diameter, 6.8 cm long), each with two zirconia balls (12.7 mm diameter) were loaded with CCSP precursor. Then the ball mill was allowed to run for 10 h.

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